Are indices (indexes) defined as UNIQUE case sensitive in MySQL?
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As per popular demand, maybe you should update the chosen answer. – Camilo Martin Jan 19 '13 at 14:00
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It depends on the collation of the field - if it's ci
(case insensitive) or cs
(case sensitive). The unique index would apply accordingly.

Yves M.
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Eran Galperin
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You can make a column case-sensitive by using this syntaxis. the unique index also will be case-sensitive.
ALTER TABLE tbl_name MODIFY
col_name column_definition
[CHARACTER SET charset_name]
[COLLATE collation_name]
Example:
ALTER TABLE `tablename` MODIFY
`column` VARCHAR(100)
CHARACTER SET utf8
COLLATE utf8_bin;
Note: utf8_bin compares strings by the binary value of each character in the string.
Tested on Msql 5.5.X

Hemerson Varela
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